C-MET

C-MET: Equipment
Atomic Absorption Spectrometer
CHNS - O Analyser
Fourier Transform Infrared  Spectrometer
Gas Chromatography
Glow Discharge Optical Spectrometer (GD-OES)
High Performance Liquid Chromatography
Inductively Coupled Optical Emmission Spectrometer
Ion Chromatography
LF Impedance Analyser
Oxygen - Nitrogen Analyser
Hot Stage Polarising Microscop
Mercury Porasimeter
Potentiostat / Galavanostat
Particle Size Analyser
Scanning Electron Microscope
Thermogravimetric Analysis / SDTA
Thermal Analysis
DMA / TMA
Universal Testing Machine
X-Ray Diffractometer
X-Ray Fluorescene Spectrometer
 
 

CHNS-O ANALYZER



INTRODUCTION
CHNS-O Analyzer is an elemental analyzer dedicated to the simultaneous determination of the amount of (%) of Carbon, Hydrogen, Nitrogen, Sulphur and Oxygen contained in organic, inorganic and polymeric materials and in substances of different nature and origin i.e. solid, liquid and gaseous samples. Technique used is DYNAMIC FLASH COMBUSTION

PRINCIPLE OF OPERATION:
The sample weighed in milligrams housed in a tin capsule is dropped into a quartz tube at 1020°C with constant helium flow (carrier gas). A few seconds before the sample drops into the combustion tube, the stream is enriched with a measured amount of high purity oxygen to achieve a strong oxidizing environment which guarantees almost complete combustion/oxidation even of thermally resistant substances. The combustion gas mixture is driven through an oxidation catalyst (WO3) zone, then through a subsequent copper zone which reduces nitrogen oxides and sulphuric anhydride (SO3) eventually formed during combustion on catalyst reduction to elemental nitrogen and sulphurous anhydride (SO2) and retains the oxygen excess. The resulting four components of the combustion mixture are detected by a Thermal Conductivity detector in the sequence N2, CO2, H2O and SO2. In case of oxygen which is analyzed separately, the sample undergoes immediate pyrolysis in a Helium stream which ensures quantitative conversion of organic oxygen into carbon monoxide separated on a GC column packed with molecular sieves.

CAPABILITIES:
CHNS-O analyzer can analyze up to 50 samples in operation.

SAMPLE SIZE:
0.1 TO 100 MG FOR SOLIDS AND LIQUID

MEASURING RANGE:
100PPM TO 100%

NATURE OF SAMPLE:
Organic/inorganic/metallorganic.





 
Centre for Materials for Electronics Technology